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We demonstrate the large scale exfoliation of bulk black phosphorus intofew-layers black phosphorus. We use wet-jet mill (WJM) as an industriallyscalable exfoliation technique. In order to avoid the degradation by oxidationof the exfoliated flakes, the few-layers black phosphorus is protected byfunctionalisation (with 4-bromobenzene-diazonium tetrafluoroborate) during theexfoliation process. We used the exfoliated and functionalised flakes asfillers in a polymethyl methacrylate matrix to test the mechanical endurance,obtaining an improvement in the Young modulus of 106% compared to the barepolymer. These data support the development of black phosphorus materials as2D-polymer fillers and performance-enhancers.

Single-step exfoliation and functionalization of few-layers black phosphorus and its application for polymer composites