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Measurements of the local tetragonality in Fe-C martensite at microstructurallength-scale through pattern matching of electron backscatter diffractionpatterns (EBSPs) and careful calibration of detector geometry are presented. Itis found that the local tetragonality varies within the complex microstructureby several per cent at largest and that the scatter in the axial ratio isincreased at higher nominal carbon content. At some analysis points the localcrystal structure can be regarded as lower symmetry than simple body centredtetragonal. A linear relation between the nominal carbon content and averagedlocal tetragonality measured by EBSD is also obtained, although the averagedaxial ratio is slightly below that obtained from more classical X-raydiffraction measurements.

Tetragonality of Fe-C martensite -- a pattern matching electron backscatter diffraction analysis compared to X-ray diffraction