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HighlightsAn organic solvent-assisted intercalation and collection (OAIC) approach for preparing Ti 3 C 2 T x  (MXene) was developed.    The features of OAIC approach are the low requirement for facility, gram-level preparation with remarkable yield and easy control over the dimension of Ti 3 C 2 T x  flakes.    The Ti 3 C 2 T x  flakes prepared by OAIC approach showed the outstanding capacitive and rate performance.Supplementary Information  The online version contains supplementary material available at 10.1007/s40820-021-00705-4.

An Organic Solvent-Assisted Intercalation and Collection (OAIC) for Ti3C2Tx MXene with Controllable Sizes and Improved Yield