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HighlightsA novel injectable double-layer-gel matrix is developed.    The hierarchically structured dual lipid gel matrix enables time-programmed drug delivery.    Applying a modest dose of sorafenib in advance can reeducate tumor-associated macrophages and potentiate anti-CD47 treatment.Supplementary Information  The online version contains supplementary material available at 10.1007/s40820-021-00647-x.

Time-Programmed Delivery of Sorafenib and Anti-CD47 Antibody via a Double-Layer-Gel Matrix for Postsurgical Treatment of Breast Cancer