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HighlightsA flexible piezoelectric nanogenerator (PENG) based on 2D single-layer MoSe 2  flake on polyethylene terephthalate was fabricated.    A high-performance flexible poly(vinyl alcohol)/MXene (PVA/MXene)-based humidity sensor was fabricated by electrospinning.    The PVA/MXene composite-based humidity sensor was self-powered by MoSe 2  PENG and exhibited excellent properties.Supplementary Information  The online version contains supplementary material available at(10.1007/s40820-020-00580-5)

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Electrospinning of Flexible Poly(vinyl alcohol)/MXene Nanofiber-Based Humidity Sensor Self-Powered by Monolayer Molybdenum Diselenide Piezoelectric Nanogenerator