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HighlightsA pH/ROS cascade-responsive carrier-free nanodrug with self-targeting activation and ROS regeneration abilities.    On-demand release of VES in response to intracellular ROS to accelerate drug release via positive-feedback loop.    Highly synergistic therapeutic efficiency via orchestrated cooperation of oxidation-chemotherapy.Electronic supplementary material  The online version of this article (10.1007/s40820-020-00492-4) contains supplementary material, which is available to authorized users.

Tumor Microenvironment Cascade-Responsive Nanodrug with Self-Targeting Activation and ROS Regeneration for Synergistic Oxidation-Chemotherapy