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HighlightsA novel N-doped strategy of C 2 N 3  −  in situ trimerization between the 2D MXene interlayers was first proposed.    The ultra-fast pseudocapacitive behavior of Ti 3 C 2 T  x  /Na 3 TCM anode was managed and verified.    The as-fabricated sodium-ion capacitor delivers excellent electrochemical performance by anode/cathode mass matching.Electronic supplementary material  The online version of this article (10.1007/s40820-020-00473-7) contains supplementary material, which is available to authorized users.

A Novel Strategy of In Situ Trimerization of Cyano Groups Between the Ti3C2Tx (MXene) Interlayers for High-Energy and High-Power Sodium-Ion Capacitors