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HighlightsA strong interfacial chemical interaction between the NiSe 2  nanocrystal and Ti 3 C 2 T  x   MXene nanosheet (NiSe 2 /Ti 3 C 2 T  x  ) was established by wrapping NiSe 2  octahedral crystal with ultrathin Ti 3 C 2 T  x   MXene nanosheet.    NiSe 2 /Ti 3 C 2 T  x   hybrid exhibits excellent performance and cycling stability both in supercapacitor and hydrogen evolution reaction.    NiSe 2  nanocrystals are stabilized by the covering of Ti 3 C 2 T  x   MXene nanosheet which served as a protective layer from its oxidation.Electronic supplementary material  The online version of this article (10.1007/s40820-019-0261-5) contains supplementary material, which is available to authorized users.

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Ultrathin Ti3C2Tx (MXene) Nanosheet-Wrapped NiSe2 Octahedral Crystal for Enhanced Supercapacitor Performance and Synergetic Electrocatalytic Water Splitting