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HighlightsCoral-like yolk–shell-structured nickel oxide/carbon composite microspheres were synthesized.    Phase separation and polystyrene nanobead decomposition affected the structure formation.    Coral-like yolk with interconnected mesopores provided excellent Li-ion storage properties.Electronic supplementary material  The online version of this article (10.1007/s40820-018-0234-0) contains supplementary material, which is available to authorized users.

Coral-Like Yolk–Shell-Structured Nickel Oxide/Carbon Composite Microspheres for High-Performance Li-Ion Storage Anodes