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Lithium-manganese orthosilicate powders were synthesized via a modified solvothermal method. Three different weight ratios of sucrose used as a carbon source were investigated for finding an effective carbon coating process. Synthesized materials were analyzed by structural and morphological (X-ray powder diffraction, scanning electron microscopy, N 2  adsorption/desorption, thermogravimetry analysis) and electrochemical (chronopotentiometry, cyclic voltammetry) methods. By increasing the sucrose content, the electrochemical performance improvement of lithium-manganese orthosilicate powder was observed, such as an increase in its specific capacity (132%) and cyclability (5%) compared with uncoated sample. The enhancement in Li 2 MnSiO 4  performance is related to an increase in its electrical conductivity and enlargement in the electrochemically active surface area due to carbon coating process.

Structure, Morphology, and Electrochemical Properties of Carbon-Coated Lithium-Manganese Orthosilicate with Sucrose as a Carbon Source