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A novel method based on vacuum-assisted sorbent extraction (VASE) used with gas chromatography-mass spectrometry (GC-MS) for isolation of volatile phenols was described. The method is based on extraction of analytes into sorbent traps (sorbent pen) filled with Tenax in a vacuum system—vials with traps from which air was evaluated. The method was applied for extraction of volatile phenols from aqueous matrix and smoked beer was used as a food example. Methyl-, dimethyl-, and trimethylphenols, along with 4-ethylphenol, 4-methylguaiacol, 4-ethylguaiacol, 4-propylguaiacol, and eugenol, were used in method development. Optimal extraction parameters were elaborated. For the analysis of volatile phenols in beer matrix, the method was characterized with satisfactory linearity (r2 ≥ 0.99) in a range of 0.005–0.5 mg/L. Limits of detection (LODs) for analyzed compounds ranged from 0.0006 to 0.018 mg/L and repeatability for majority of compounds was < 5% for a single trap extraction. The detected volatile phenols in beer samples ranged from 0.003 to 0.672 mg/L.

Use of Sorbent-Based Vacuum Extraction for Determination of Volatile Phenols in Beer