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A hybrid co-continuous network embedding nanoparticles (maximum 1.25 nm in size) was obtained;A post-cure was performed above the glass transformation temperature, Tg, of neat epoxy;The post cure makes Tg, storage modulus and Heat Release Rate (HRR) to increase;No dripping in flame test and up to 40% HRR reduction for only 2 wt.% silica content is observed;The post cure effects depend on nanoparticles clustering in the glass transformation range.

Effects of post cure treatment in the glass transformation range on the structure and fire behavior of in situ generated silica/epoxy hybrids