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Since the late 1960s, ceric hydrogen phosphates have attracted the attentionof scientists due to remarkable ion exchange, sorption, proton-conduction andcatalytic properties. In this work, through the application of varioussolvents, we, for the first time, have obtained monolithic aerogels based onceric hydrogen phosphates with high porosity (~99%) and extremely low density(~10 microg/cm3). The composition and structure of aerogels were thoroughlystudied with XRD, TEM, SEM, XPS, low temperature nitrogen adsorption methods,TGA/DSC, Fourier-transform infrared spectroscopy (FTIR) and small-angle neutronscattering (SANS). The aerogels were found to belong to the fibrous macroporousaerogels family.

First rare-earth phosphate aerogel: sol-gel synthesis of monolithic ceric hydrogen phosphate aerogel