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In this work, two Tc radiochemical isolation methods—a conventional method by Triskem TEVA ®  resin and a rapid method by Empore™ Tc Rad Disk—are compared in the field of nuclear decommissioning and  99 Tc assessment. The conventional method results more selective than the rapid one, being able to remove almost 100% of the main radiological interferers with the exception of the  90 Y; however, the rapid method obtains higher chemical yields (97% vs. 80%) and slightly lower detection limits (0.025 Bq vs. 0.030 Bq) than the conventional. Both methods are similar with regards to equipment and reagent costs.

Selectivity analysis of 99Tc determination by LSC in the field of nuclear decommissioning