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Coordination circumstance of neptunyl ion in concentrated CaCl[2] solutions was analyzed by Raman spectrometry. Besides the symmetric stretch (ν[1]) mode of NpO[2](+) and NpO[2](2+), the asymmetric stretch (ν[3]) mode of NpO[2](+) was found. The Raman intensity of the ν[3] mode increased with the concentration of CaCl[2] in the system. This would be attributable to the cation–cation interaction between Np(V) and Ca(II)

Raman spectroscopic study on NpO2 +–Ca2+ interaction in highly concentrated calcium chloride