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A new coordination polymer [Cd(μ-OH)()(bipy)] (). ( = 1,2-naphthalene dicarboxylate, bipy = 4,4′-bipyridine), was obtained under hydrothermal condition. The structure of  has been determined by single-crystal X-ray diffraction analysis and further characterized by elemental analysis and IR spectrum. Single-crystal X-ray diffraction analyses reveal that complex  crystallizes in triclinic system, ī space group. Complex  possesses a 3D pcu net based on a pentanuclear Cd(II) cluster. Each pentanuclear Cd(II) cluster links with neighboring ones and generates a rod-shaped secondary building unit, which is further extended by bipy ligands to forms a three-dimensional network. Furthermore, the luminescent properties of this complex and the free ligand have been investigated. Complex  can be excited directly and emit strong soild-state fluorescence at room temperature, which may make them excellent candidates for fluorescent materials.

A New 3D Coordination Polymer Based on Pentanuclear Cd(II) Rod-Shaped Secondary Building Unit: Synthesis, Crystal Structure and Luminescent Property