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Multiferroic ( x )BaTiO 3 /(1 −  x )Li 0.5 Fe 2.5 O 4  (0.0 ≤  x  ≤ 1) perovskite/spinel nanocomposite was synthesized using a modified citrate auto-combustion method. Both BaTiO 3  (BTO) and Li 0.5 Fe 2.5 O 4  (LFO) phases along with their composites were successfully characterized using X-ray diffraction, Fourier transformation infrared spectroscopy, and X-ray absorption fine structure spectroscopy. The nanoscale, morphology, and magnetic properties were imaged and acquired using high resolution transmission electron microscopy, atomic force microscopy, and vibrating sample magnetometer. Synchrotron radiation-based elemental selective XAFS technique was performed around Fe  K -edge to obtain the selective and the detailed local structural information of Li 0.5 Fe 2.5 O 4  nanoparticles (NPs). The main remarkable result in this work is the enhancement in the coercivity ( H  C ) of LFO NPs after compositing with BTO particularly at  x  = 0.6, and at  x  = 0.8. Based on the collected results, BTO/LFO nanocomposite can be seen as a good candidate for different technological applications including magnetically modulated piezoelectric, safety rechargeable batteries, and multilayer ceramic capacitor.

Optimization of magnetic properties of BaTiO3/Li0.5Fe2.5O4 multiferroics prepared via modified low-temperature combustion