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A glass-forming domain is found and studied within Bi 2 O 3 -Sb 2 O 3 -TeO 2 system. The glasses composition were obtained in pseudo-binary x SbO 1.5 , (1- x )TeO 2 for 0.05 ≤  x  ≤ 0.20. The constitution of glasses in the system Sb 2 O 3 -TeO 2 was investigated by DSC, Raman, and Infrared spectroscopy. The influence of a gradual addition of the modifier oxides on the coordination geometry of tellurium atoms has been elucidated based Infrared and Raman studies and showed the transition of TeO 4 , TeO 3+1 , and TeO 3 units with increasing Sb 2 O 3 content. XRD results reveal the presence of three crystalline: γ-TeO 2 , α-TeO 2 , and SbTe 3 O 8 phases during the crystallization process. The density of glasses has been measured. The investigation in the ternary system by the solid state reaction using XRD reveals the existence of a solid solution Bi 1- x  Sb 1- x  Te 2 x  O 4 isotopic to BiSbO 4 with 0 ≤  x  ≤ 0.1.

Glasses formation, characterization, and crystal-structure determination in the Bi2O3–Sb2O3–TeO2 system prepared in an air