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Silyl- and phenylacetylenes undergo efficient homodimerization in the presence of a second generation Grubbs catalyst. The reaction permits fully regio- and stereoselective synthesis of disubstituted 1,3-enynes. The other commonly used ruthenium-based olefin metathesis catalysts remain inactive in the reaction.Graphical Abstract

Regio- and Stereoselective Homodimerization of Monosubstituted Acetylenes in the Presence of the Second Generation Grubbs Catalyst