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Summary  Oxalic acid excretion was measured in nine patients receiving methoxyflurane and six patients receiving halothane. Oxalic acid excretion increased from 5 to 23 times in the immediate postoperative period in patients receiving methoxyflurane, whereas no increase was noted in those receiving halothane. Despite the striking increase in oxalic acid excretion, no alteration in renal function and no polyuric state developed. The renal failure that occasionally develops after methoxyflurane anaesthesia appears to be multifactorial in origin and a hyperoxaluric state may play a role in some instances.

Oxalic acid excretion after methoxyflurane and halothane anaesthesia