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The local order around molybdenum and tungsten atoms in various sodium molybdophosphate and sodium tungstophosphate glasses has been investigated using extended X-ray absorption fine structure (EXAFS). Both molybdenum and tungsten atoms are present in six-coordinated environment in these glasses. Magic angle spinning nuclear magnetic resonance (MAS NMR) of31P suggests that metaphosphate or neutral [POO3/2] groups are present in these glasses.

EXAFS and MAS NMR studies of sodium molybdophosphate and sodium tungstophosphate glasses