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Ü b e r A n r e g u n g ( l e s H e r r n P r o f . D r . W . G i n t l b a t d e r E i n e v o n u n s b e r e i t s v o r l ä n g e r e r Z e i t V e r s u c h e a n g e s t e l l t , w e l c h e d e n Z w e c k h a t t e n , d a r z u t h u n , o b s i c h n i c h t a u f e x p e r i m e n t e l l e m W e g e e i n e V e r s c h i e d e n h e i t i n d e m B i n d u n g s v e r h ä l t n i s s e d e r d r e i C h l o r  a t o m e d e s P h o s p h o r o x y c h l o r i d s n a c h w e i s e i l l a s s e . N a c h d e m d i e s e v o r l ä u f i g e n V e r s u c h e d i e R e a k t i o n s f ä h i g k e i t d i e s e r V e r b i n d u n g g e g e n M e t a l l e d a r g e t h a n h a t t e n , w u r d e e i n e U n t e r s u c h u n g d e r h i e b e i v e r l a u f e n d e n P r o c e s s e v o n u n s g e m e i n s a m u n t e r n o m m e n . D a s P h o s p h o r o x y c h l o r i d , w e l c h e s w i r v e r w e n d e t e n , w u r d e m e h r e r e M a l e f r a c t i o n i r t u n d n u r d i e P a r t i e v o n n o r m a l e m S i e d e p u n k t b e n u t z t . D u r c h P r ü f u n g e i n e r k l e i n e n M e n g e m i t Z n u n d N a w u r d e d i e A b w e s e n h e i t v o n C 1 H c o n s t a t i r t . D i e V e r s u c h e w u r d e n s o a n g e s t e l l t , d a s s d i e M e t a l l e u n d d a s C h l o r i d i n R ö h r e n e i n g e s c h m o l z e n a u f v e r s c h i e d e n e T e m p e r a t u r e n e r h i t z t w u r d e n . W i r l a s s e n n u n z u n ä c h s t d i e R e s u l t a t e d e r e i n z e l n e n V e r s u c h e f o l g e n .

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