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The Raman spectra of cadmium bromide solutions with bromide to cadmium mole ratios varying from 1.0 to 9.74 were studied at 200°C. Factor analysis revealed that three complexes contributed to the spectra. From a comparison with previous results at 25°C these species were identified as CdBr2, CdBr3-, and CdBr42- cadmium existed as the tetrabromo complex, CdBr42-, at mole ratios greater than 5.99. A formation constant of 7±2 was determined for CdBr42- at 200°C. No evidence of Cd(H2O)62+ or CdBr+ was found, although electroneutrality dictates that one or both of these species must exist at low mole ratios.

journal of solution chemistry

Vibrational spectral studies of solutions at elevated temperatures and pressures. X. Raman spectral study of aqueous cadmium bromide solutions at 25 and 200�C