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The microstructure of a CoNiAl FSMA was determined by conventionaltransmission electron microscopy, electron diffraction studies together withadvanced microscopy techniques and in-situ Lorentz microscopy. 10 to 60 nmsized rod-like precipitates of hcp $\epsilon$-Co were confirmed to be presentby HRTEM. The orientation relationship between the precipitates and B2 matrixis described by the Burgers orientation relationship. The crystal structure ofthe martensite obtained after cooling is tetragonal L10 with a (1-11) twinningplane. The magnetic domain structure was determined during an in-situ coolingexperiment using the Fresnel mode of Lorentz microscopy. While transformationproceeds from B2 austenite to L10 martensite, new domains are nucleated leadingto a decrease in domain width, with the magnetization lying predominantly alonga single direction. It was possible to completely describe the relationshipbetween magnetic domains and crystallographic directions in the austenite phasethough complications existed for the martensite phase.

Microstructure of precipitates and magnetic domain structure in an annealed Co38Ni33Al29 shape memory alloy