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Nanostructured Fe40Ni40P14B6 alloys ingots of diameter 3~5 mm could besynthesised by a metastable liquid state spinodal decomposition method. Themolten Fe40Ni40P14B6 alloy was purified by means of the fluxing technique andthus a large undercooling could be achieved. For undercooling Delta T > 260 K,the microstructure of the undercooled specimen had exhibited liquid statespinodal decomposition in the undercooled liquid state. The microstructurecould be described as two intertwining networks with small grains dispersed inthem. For undercooling Delta T > 290 K, the overall microstructure of thespecimen changed into a granular morphology. The average grain sizes of thesmall and large grains are ~ 30 nm and ~ 80 nm, respectively. These preparedsamples are soft magnets with saturation magnetization Bs ~0.744 T.

Formation of bulk ferromagnetic nanostructured Fe40Ni40P14B6 alloys by metastable liquid spinodal decomposition