Open AccessStructural, Optical and Thermal Characterization of Synthesised Heterocyclic Organic Compound
Author(s) -
Arpitha Kumari,
Ganesh Sanjeev,
Boja Poojari,
P. V. Soumya
Publication year - 2021
Publication title -
asian journal of physical and chemical sciences
Language(s) - English
Resource type - Journals
ISSN - 2456-7779
DOI - 10.9734/ajopacs/2021/v9i430142
Subject(s) - thermogravimetric analysis , thermal stability , characterization (materials science) , fourier transform infrared spectroscopy , differential thermal analysis , materials science , thermal analysis , fluorescence , crystal structure , condensation reaction , analytical chemistry (journal) , chemistry , nuclear chemistry , thermal , crystallography , organic chemistry , chemical engineering , nanotechnology , optics , diffraction , physics , meteorology , engineering , catalysis
A heterocyclic organic compound of 3-[(2z)-2-methyl-3-(4-nitrophenyl) prop-2-enoyl]-2H-(1-benzopyran-2-one) (MNB) is synthesized using Claisen-Schmidth condensation reaction. Structural characterization and presence of functional groups are carried out using powder X-ray diffractogram and FTIR spectroscopic studies respectively. Thermogravimetric analysis and differential thermal analysis are carried out to determine the melting property and it shows good thermal stability among organic crystal showing result at 166°C. Second Harmonic Generation efficiency study is carried out using Nd: YAG laser, this revealed that titled compound is good for NLO characterization and applicable in optoelectronics. PL wavelength present in visible region conclude that sample shows fluorescence property.