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Reductive ozonolysis of soybean oil: Laboratory optimization of process variables
Author(s) -
Throckmorton P. E.,
Pryde E. H.
Publication year - 1972
Publication title -
journal of the american oil chemists' society
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.512
H-Index - 117
eISSN - 1558-9331
pISSN - 0003-021X
DOI - 10.1007/bf02609377
Subject(s) - ozonolysis , acetal , organic chemistry , acetic acid , chemistry , solvent , catalysis , soybean oil , charcoal , food science
Statistically designed experiments were carried out to determine the effect of reaction variables in the reductive ozonolysis of soybean oil to azelaaldehydic glyceride methyl acetal. Yields of this acetal were essentially quantitiative under optimum conditions, which include a 1:1 mixture of acetic acid and butanol as solvent, a solvent‐oil ratio of 1.5:1, and hydrogenation at 150 psig and 50 C with palladiumon‐charcoal catalyst.
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