Premium
The synthesis and purification of pentylenetetrazole‐10‐ 14 C
Author(s) -
Stiver J. F.,
Data J. B.,
Christian J. E.
Publication year - 1970
Publication title -
journal of labelled compounds
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0022-2135
DOI - 10.1002/jlcr.2590060106
Subject(s) - sublimation (psychology) , chemistry , liquid scintillation counting , chromatography , cyclohexanone , thin layer chromatography , radiochemistry , nuclear chemistry , organic chemistry , psychology , psychotherapist , catalysis
Pentylenetrazole‐10‐ 14 C was synthesized by reacting hydrazoic acid with cyclohexanone‐1‐ 14 C. Purification was carried out using sublimation and thick layer chromatography. Proof of radiochemical purity was determined using thin layer chromatography and autoradiography. The specific activity was found using liquid scintillation counting.