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The synthesis of L‐ 14 C‐serine ethanolamine phosphate, L‐Serine 1,2‐ 14 C‐ethanolamine phosphate, L‐ 3 H‐Serine 1,2‐ 14 C‐ethanolamine phosphate, and related compounds
Author(s) -
Porcellati G.
Publication year - 1967
Publication title -
journal of labelled compounds
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0022-2135
DOI - 10.1002/jlcr.2590030405
Subject(s) - serine , ethanolamine , threonine , phosphate , chemistry , biochemistry , stereochemistry , phosphorylation
A procedure for the chemical synthesis of the following labelled phosphodiesters : L‐ 14 C‐serine ethanolamine phosphate, L‐serine 14 C‐ethanolamine phosphate, L‐ 3 H‐serine 14 C‐ethanolamine phosphate, L‐ 14 C‐threonine ethanolamine phosphate, L‐threonine 14 C‐ethanolamine phosphate, L‐ 14 C‐serine L‐ 14 C‐serine phosphate and L‐ 14 C‐threonine L‐ 14 C‐threonine phosphate is reported. The variously labelled forms of these phosphodiesters have been synthesized and purified by a route and a procedure leading to unequivocal structures for the products. The labelled L‐serine L‐serine phosphate and L‐threonine L‐threonine phosphate have been obtained as by‐products in the preparation of the labelled forms of L‐serine ethanolamine phosphate and L‐threonine ethanolamine phosphate, respectively.