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Synthesis of tributyltin‐113 benzoate
Author(s) -
Otto P. Ph. H. L.,
Creemers H. M. J. C.,
Luijten J. G. A.
Publication year - 1966
Publication title -
journal of labelled compounds
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0022-2135
DOI - 10.1002/jlcr.2590020402
Subject(s) - tributyltin , tin , yield (engineering) , isotopes of tin , antimony , chemistry , methyl benzoate , nuclear chemistry , radiochemistry , isotope , organic chemistry , materials science , metallurgy , physics , quantum mechanics
Tributyltin‐113 benzoate was prepared from tin metal labelled with tin‐113, by a three step synthesis, with a chemical yield of 37%. The radio‐chemical yield was 22%. The amount of tributyltin‐113 benzoate prepared was 1.3 g, the specific activity 0.7 mC/gram, and the radiochemical purity 98.9%. Apart from Sn‐113 no other gamma‐emitting tin isotopes were present, neither did antimony radio‐isotopes occur.