Premium
Deiodination reactions using tributyltin hydride for potential labelling experiments
Author(s) -
Zippi Elizabeth M.,
Plourde Gary W.,
Satyamurthy N.
Publication year - 1995
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580360408
Subject(s) - iodobenzene , chemistry , tributyltin hydride , tributyltin , labelling , hydride , radiochemistry , organic chemistry , catalysis , biochemistry , hydrogen
Abstract 2,6‐Dinitro‐1‐iodobenzene and 2,4‐dinitro‐1‐iodobenzene were deiodinated with tributyltin hydride at different temperatures using various addition modes. The product ratios of 1,3‐dinitrobenzene and the corresponding tributylstannyldinitrobenzene compounds were determined by NMR in order to evaluate the optimum conditions for impending tritiation experiments.