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The preparation of high purity H 2 35 S
Author(s) -
Collins C. D.,
Bell J. N. B.
Publication year - 1994
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580341116
Subject(s) - chemistry , yield (engineering) , catalysis , nuclear chemistry , radiochemistry , pumice , organic chemistry , metallurgy , materials science , volcano , seismology , geology
H 2 35 S was synthesised by the reaction of H 2 with elementary [ 35 S] sulphur at 600°C with 100 mg of pumice added as a catalyst. The resulting gas was purified by placing the preparation vessel in a pack of ice. A yield of 46% was produced.