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Facile synthesis of (4 S )‐(−)‐[9‐ 3 H]limonene
Author(s) -
Hiraga Yoshikazu,
Danjo Hiroshi,
Ito Takatoshi,
Suga Takayuki
Publication year - 1993
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580330809
Subject(s) - chemistry , limonene , stereochemistry , organic chemistry , combinatorial chemistry , chromatography , essential oil
(4 S )‐[9‐ 3 H]‐1‐Methyl‐4‐(1′‐methylethenyl)cyclohexene ((4 S )‐(−)‐[9‐ 3 H]limonene) was synthesized from (1′ S ,2 RS )‐2‐(4′‐methylcyclohex‐3′‐enyl)porpanal ((4 S ,8 RS )‐(−)‐1‐ p ‐menthen‐9‐al) via a convenient route in a high yield with improved enantiomeric purity.