Premium
Preparation of 15 N labeled tetranitromethane C( 15 NO 2 ) 4
Author(s) -
Skawinski William,
Flisak Joseph,
Chung Alex C.,
Jordan Frank,
Mendelsohn Richard
Publication year - 1990
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580281010
Subject(s) - tetranitromethane , chemistry , nitric acid , anhydrous , acetic anhydride , tyrosine , acetic acid , nitration , radiochemistry , nuclear chemistry , medicinal chemistry , organic chemistry , biochemistry , catalysis
15 N labeled tetranitromethane, C( 15 NO 2 ) 4 , was prepared from anhydrous nitric acid and acetic anhydride. A procedure for the preparation of the nitric acid from Na 15 NO 3 is described. Tyrosine was nitrated with H 15 NO 3 and its 15 N NMR spectrum compared well with that of tyrosine nitrated with C( 15 NO 2 ) 4 .