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Geminally 13 c‐labelled vinyl iodides; E ‐2′‐iodo‐4‐methoxyphenyl[2′‐ 13 C]ethene from [ 13 C]iodoform
Author(s) -
Baker Karen V.,
Brown John M.,
Cooley Neil A.
Publication year - 1988
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580251109
Subject(s) - iodoform , chemistry , acetophenone , carbon 13 nmr , derivative (finance) , chromium , organic chemistry , medicinal chemistry , nuclear chemistry , catalysis , financial economics , economics
Abstract [ 13 C]Iodoform has been synthesised from [ 13 C]acetophenone and converted into the title compound by preparation of its chromium [III] derivative and reaction with 4‐methoxybenzaldehyde. Purification was effected by recrystallisation from MeOH, or silica chromatrography.