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Synthesis of deuterium labelled clofibrate
Author(s) -
Saljoughian Manouchehr
Publication year - 1984
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580210912
Subject(s) - chemistry , clofibrate , deuterium , labelling , recrystallization (geology) , acetone , distillation , tritium , radiochemistry , chromatography , organic chemistry , nuclear physics , biochemistry , physics , paleontology , biology
The synthesis of deuterium labelled clofibrate using fully deuterated acetone, (CD 3 ) 2 CO, as labelling agent is described. Purification of labelled material was accomplished by recrystallization and fractional distillation.