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Synthesis of 14 C‐labelled methylazoxymethanol acetate of high specific activity
Author(s) -
Cazer Frederick D.,
Barnela Satish B.,
Kumar Kultar S.,
Kamat Prabhakar L.,
Milo George E.,
Witiak Donald T.
Publication year - 1984
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580210109
Subject(s) - chemistry , yield (engineering) , specific activity , radiochemistry , nuclear chemistry , organic chemistry , enzyme , materials science , metallurgy
The micro‐scale synthesis of 14 C‐labelled methylazoxymethanol acetate ( 14 C‐MAM‐acetate) having a specific activity of 110 mCi/mmol was accomplished in 25% yield from N,N′‐[methyl‐ 14 C] ‐dimethylhydrazine with a specific activity of 112.5mCi/mmol.