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Synthesis of 14 C‐labeled indole‐3‐acetylaspartic acid
Author(s) -
Cohen Jerry D.
Publication year - 1981
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580180916
Subject(s) - chemistry , indole test , aspartic acid , indole 3 acetic acid , acetic acid , nuclear chemistry , stereochemistry , medicinal chemistry , organic chemistry , biochemistry , amino acid , auxin , gene
The synthesis of indole‐3‐acetyl‐2‐ 14 C‐N‐aspartic acid from carrier‐free indole‐3‐acetic acid‐2‐ 14 C (54.5 mCi/mmole) and bis‐t‐butyl‐l‐aspartic acid was accomplished by coupling with dicyclohexylcarbodiimide followed by removal of the ester blocking groups by treatment with 2 N NaOH.