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Syntheses of astato compounds by melt method
Author(s) -
Shiue C.Y.,
Meyer G.J.,
Ruth T. J.,
Wolf A. P.
Publication year - 1981
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580180715
Subject(s) - chemistry , chromatography , organic chemistry , nuclear chemistry
m‐Astatobenzoic acid (2) methyl m‐astatobenzoate (3), and m‐astatohippuric acid (4) were synthesized by the melt method. Reaction of methyl m‐bromobenzoate with astatide at 200°C gave methyl m‐astatobenzoate. Compounds 2 and 4 were synthesized by similar method. Compounds 2 and 3 were purified and identified by radio‐gaschromatography.