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Darstellung von N ‐Alkyliminobis(thiocarbaldehyden)
Author(s) -
Allenstein Eckhard,
Sille Falk,
Stegmüller Bruno
Publication year - 1979
Publication title -
liebigs annalen der chemie
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.825
H-Index - 155
eISSN - 1099-0690
pISSN - 0170-2041
DOI - 10.1002/jlac.197919790710
Subject(s) - chemistry , adduct , antimony , hydrogen sulfide , medicinal chemistry , hydrogen chloride , chloride , sulfide , polymer chemistry , organic chemistry , sulfur
Preparation of N ‐Alkyliminobis(thiocarbaldehydes) N ‐Methyl‐ ( 2a ) and N ‐ethyliminobis(thiocarbaldehyde) ( 2b ), and their hydrochlorides 4 , were prepared by reaction of the corresponding N ‐alkylbis(dichloromethyl)amines 3 with hydrogen sulfide. Their properties and spectroscopic data are reported. Compound 2a reacts with antimony(V) chloride to give a 1:1 adduct.
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