13 C‐NMR INADEQUATE Spectrum with Broad Band Decoupling by Supercycles | Zendy

Bolte Peter | Zendy; Klessinger Martin | Zendy; Wilhelm Konrad | Zendy

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13 C‐NMR INADEQUATE Spectrum with Broad Band Decoupling by Supercycles

Author(s) -

Bolte Peter,

Klessinger Martin,

Wilhelm Konrad

Publication year - 1984

Publication title -

angewandte chemie international edition in english

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 0570-0833

DOI - 10.1002/anie.198401521

Subject(s) - decoupling (probability) , coupling constant , pulse sequence , spectral line , physics , proton , measure (data warehouse) , spectrum (functional analysis) , chemistry , nuclear magnetic resonance , quantum mechanics , computer science , data mining , engineering , control engineering

The informational value of 13 C‐ 13 C coupling constants has hardly yet been exploited, because they were extremely difficult to measure in molecules with 13 C in natural abundance. Use of the “incredible natural abundance double quantum transfer experiment” method improves the situation. The combination of this method with an effective pulse sequence for proton decoupling now permits routine measurement of J ( 13 C, 13 C).

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