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Fast and accurate multi-residue pesticides inspecting method needs in Agro-Fishery ProductsInspection Center. So, We tried to seek the optimum method using GC-TOF/MS, GC-ECD, GC-NPD afterQuEChERS sample preparation. In GC-TOF/MS, 138 kinds of pesticide were spiked at 0.3 and 0.5μg/g forthe identification and quantification in lettuce sample. Recoveries of 77 pesticides were between 70 and130% with RSD (relative standard deviation lower than 20% at 0.3μg/g. In GC-ECD, NPD, 146 kinds ofpesticide were spiked for the identification and quantification in lettuce. Recoveries of 61 species werebetween 70 and 130% with lower than 20%. These results indicated that GC-TOF/MS, GC-ECD, NPDanalysis with the QuEChERS sample preparation can be partly applied to multi-residue pesticides in vegetables. Key words Multi-residue pesticides, GC-TOF/MS, ECD, NPD, QuEChERS        µg/g       . 1960  FDA   (MFDS, 2012),             (MFDS, 2012).       (Ock, 2009). 2000            QuEChERS (Anastassiades, 2003).QuEChERS Quick, Easy, Cheap, Effective, Rugged,Safe     C

Multi-residue Analysis of Pesticides using GC-TOF/MS, ECD, NPD with QuEChERS Sample Preparation