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Syntheses of the 3-O-demethyl-2,3-di-epi-fortimicins A and B and the 3-O-demethyl-3-epi-fortimicins A and B have been accomplished in processes the key steps of which were solvolyses of 4-N-acetyl-3-O-demethyl-3-O-methanesulfonylfortimicin derivatives. Antibacterial activities of the new antibiotics are reported.

3-O-demethyl-2,3-di-epi-fortimicins and 3-O-demethyl-3-epi-fortimicins.