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The structural phase transition of single crystals was investigated by determining the spin-lattice relaxation time . The number of resonance lines in the spectrum changes from seven to one near 375 K, which means that above 375 K the Cs sites are symmetric. Further, the of the nucleus undergoes a significant change near 375 K, which coincides with the change in the splitting of the resonance lines. The change in near is related to the loss of , and means that the forms of the octahedra of water molecules surrounding are disrupted.

133Cs Nuclear Magnetic Resonance Relaxation Study of the Phase Transition of Cs2MnCl4·2H2O Single Crystals

¹³³Cs Nuclear Magnetic Resonance Relaxation Study of the Phase Transition of Cs₂MnCl₄·2H₂O Single Crystals