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An ionic liquid system based on two amide anions; bis(fluorosulfonyl)amide anion (FSA) and bis(trifluoromethanesulfonyl)amide anion (TFSA), with a quaternary ammonium cation; N,N,N-trimethyl-N-propylammonium cation (TMPA+), was investigated over entire composition range. The system showed the binary phase diagram and the eutectic point was 5.5°C around the anion ratio of 1:2 (FSA: TFSA). Polymorphic behavior of solidified ionic liquid was observed by X-ray diffraction (XRD) and discussed comparing with ionic liquids composed of other anion; (fluorosulfonyl) (trifluoromethylslufonyl)amide anion (FTA−) or tetrafluoroborate anion (BF4). In addition, the phase diagram of the ionic liquid system containing lithium cation with binary anion was confirmed. Raman spectroscopy suggested that lithium cation interacts more preferentially with TFSA than FSA. © The Electrochemical Society of Japan, All rights reserved.

electrochemistry

Thermophysical Properties of Binary Amide Anion-Based Ionic Liquids; TMPAFSA&lt;i&gt;&lt;sub&gt;x&lt;/sub&gt;&lt;/i&gt;TFSA&lt;sub&gt;1−&lt;/sub&gt;&lt;i&gt;&lt;sub&gt;x&lt;/sub&gt;&lt;/i&gt;