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AMPS, POEM  GMA   , AMPS  $Li_2CO_3$         poly(POEM-co-AMPSLi-co-GMA)  . POEM  AMPS  POEM       ,       .    GMA      , 16 mol% $1.0{\times}10^{-6}S\;cm^{-1}$   . , -   2 mol%  $4.08{\times}10^{-6}S\;cm^{-1}$    ,  6 V    .     , 0.11 MPa   270%  . 【In this study, crosslinked poly(POEM-co-AMPSLi-co-GMA)s were prepared by epoxy coupling of GMA after radical copolymerization of AMPS, POEM and GMA followed by acid-base titration reaction between sulfonic acid of AMPS and $Li_2CO_3$ . It was observed that the crystalline melting temperature of POEM was effected by mol% of components and shifted to lower value by lithiation of AMPS group. The ionic conductivity of crosslinked polymer electrolyte was decreased by addition of GMA but maintained over $1.0{\times}10^{-6}S\;cm^{-1}$ until 16 mol%. Particularly, the self-doped polymer electrolyte with 2 mol% of GMA showed its ionic conductivity as high as $4.08{\times}10^{-6}S\;cm^{-1}$ at room temperature and electrochemical stability up to 6 V. In addition, 0.11 MPa of modulus and 270% of elongation were obtained from the free standing film of crosslinked polymer electrolyte.】

Synthesis of Crosslinked Poly(POEM-co-AMPSLi-co-GMA) Electrolytes and Physicochemical Properties