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Polymer electrolytes consisted of BF3LiMA and 300 (PEGMA300) or 1100 (PEGMA1100) g mol 1 of PEGMA were prepared and the electrochemical properties were char- acterized. Interestingly, the AC-impedance measurement shows 1.22 × 10 5 Sc m 1 of room tem- perature ionic conductivity from PEGMA1100 based solid polymer electrolytes while 8.54 × 10 7 Sc m 1 was observed in PEGMA300 based liquid polymer electrolytes. The more suitable coordination between lithium ion and ethylene oxide (EO) unit might be the reason of higher ionic conductivity which can be possible in PEGMA1100 based electrolytes since it has 23 EO units in monomer. The lithium ion transference number was found to be 0.6 due to the side reactions between BF3 and lithium metal expecially for longer time but 0.9 was observed within 3000 seconds of measuring time which is strong evidence of a single-ion conductor.

Synthesis of Self-doped Poly(PEGMA-co-BF3LiMA) Electrolytes and Effect of PEGMA Molecular Weight on Ionic Conductivities

Synthesis of Self-doped Poly(PEGMA-co-BF₃LiMA) Electrolytes and Effect of PEGMA Molecular Weight on Ionic Conductivities