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C JHP – Vol. 69, No. 4 – July–August 2016 JCPH – Vol. 69, no 4 – juillet–août 2016 The forced degradation experiments resulted in recovery of 10.3% and 34.5% of the amlodipine signal in acidic conditions and oxidative conditions, respectively. Amlodipine retention time was about 4.4 min, and the peak for amlodipine was clearly separated from peaks for excipients and degradation products, which all eluted between 0.9 and 3.8 min. Throughout the stability study, all of the suspensions could be easily resuspended. No notable change in colour or odour was observed. Formulations prepared from bulk amlodipine besylate and from tablets and stored at 5°C maintained not less than 90% of their initial concentration after 90 days (Tables 1 and 2). With storage at 25°C, preparations made from bulk powder remained stable for 60 days in both types of storage container, whereas formulations prepared from tablets were stable for 60 days in bottles and 45 days in syringes. In conclusion, amlodipine besylate suspensions equivalent to 1 mg/mL of amlodipine base in Oral Mix prepared from bulk powder were stable for up to 90 days at 5°C (98.1% remaining in bottles and 97.3% remaining in syringes) and 60 days at 25°C (92.1% remaining in bottles and 91.5% remaining in syringes). Suspensions prepared from tablets were also stable for 90 days at 5°C (99.0% remaining in bottles and 100.0% remaining in syringes), but with storage at 25°C, these suspensions were stable for only 60 days in bottles (94.2% remaining) and 45 days in syringes (91.0% remaining). These results are comparable to the results obtained by Nahata and others5 using other aqueous vehicles.

Stability of Hydrocortisone, Nifedipine, and Nitroglycerine Compounded Preparations for the Treatment of Anorectal Conditions