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A series of novel 3-azolylpyrazolo[5,1-c][1,2,4]triazines was synthesized by reaction of 3-substituted pyrazole-5-diazonium salts with β-azolyl enamines in an efficient fashion. The structures of the compounds prepared were characterized by NMR spectroscopy, massspectrometry, elemental and X-ray diffraction analyses. Plausible mechanisms were formulated.

Reactivity of 3-substituted pyrazole-5-diazonium salts towards 3-azolyl enamines. Synthesis of novel 3-azolylpyrazolo[5,1-c][1,2,4]triazines