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The synthesis of either monoor bis-adducts via Michael reaction between active methyl ne compounds and α,β-unsaturated reagents is reported. These processes are catalyzed by two heterogeneous basic catalysts, namely KG-NEt 2 and KG-TBD. Both catalysts show good catalytic efficiency and can be reused several time s fully preserving their efficiency. The process could be efficiently performed under continuous flo w conditions obtaining promising results in term of yield and selectivity.

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Triethylamine and TBD supported on silica: useful heterogeneous catalysts for the reaction of β-dicarbonyl derivatives with α,β-unsaturated compounds under batch and continuous flow conditions